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In the title mol­ecule, C21H19NO4, the piperidine ring adopts a chair conformation. The benzoyl group has a bis­ectional orientation. The planar furyl rings and the methyl group each have an axial orientation. The structure is stabilized by inter- and intra­molecular C—H⋯O hydrogen bonds.

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In the title compound, C22H21NO5S, the 2-naphthol group and the thio­phene ring are almost coplanar, with a dihedral angle of 5.75 (7)°. The structure is stabilized by intra­molecular O—H⋯O, O—H⋯N and C—H⋯S, and inter­molecular C—H⋯O hydrogen-bonding inter­actions.

 · C6. 0.1 M Bicine pH 9.0, 20% PEG 6000 D1. 0.1 M Citric Acid pH 4.0, 30% PEG 6000 D2. 0.1 M Citric Acid pH 5.0, 30% PEG 6000 D3. 0.1 M MES pH 6.0, 30% PEG 6000 D4. 0.1 M HEPES pH 7.0, 30% PEG 6000 D5. 0.1 M Tris pH 8.0, 30% PEG 6000 D6. 0.1 M Bicine pH 9.0, 30% PEG 6000 Well A1. 0.1 M Citric Acid pH 4.0, 5% PEG 6000

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In the title compound, C14H14N2O2, the angle between the mean plane of the N-methyl-3-nitro­aniline system (r.m.s. deviation = 0.0185 Å) and the p-tolyl unit is 89.79 (4)°. In the crystal, hydrogen-bonded chains running along [10-1] are generated by the linking of neighbouring mol­ecules via N—H⋯O and C—H⋯O hydrogen bonds involving the 3-nitro­aniline systems and forming R22(8 ...

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The title Schiff base compound, 4-nitro-1-oxo-2-{(E)-[2-(piperidin-1-yl)eth­yl]iminiometh­yl}cyclo­hexa­dienide, C14H19N3O3, exists as a zwitterion, with the H atom of the phenol group being transferred to the imine N atom. The C=O, CAr—CAr and C—N bond lengths are in agreement with the oxocyclo­hexa­dienide–iminium zwitterionic form.

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 · C3. 0.1 M MES pH 6.0, 1.0 M Lithium Chloride, 20% PEG 6000 C4. 0.1 M HEPES pH 7.0, 1.0 M Lithium Chloride, 20% PEG 6000 C5. 0.1 M Tris pH 8.0, 1.0 M Lithium Chloride, 20% PEG 6000 C6. 0.1 M Bicine pH 9.0, 1.0 M Lithium Chloride, 20% PEG 6000 D1. 0.1 M Citric Acid pH 4.0, 1.0 M Lithium Chloride, 30% PEG 6000 D2.

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The title compound, C12H19O4P, has a distorted tetra­hedral geometry around the P atom. The molecules form dimers with R22(10) ring motifs due to inter­molecular O—H⋯O hydrogen bonds. The double-bonded O atom of the phospho­nate group behaves as an acceptor and the hydr­oxy group acts as a donor. Both of the ethyl groups are disordered with occupancies of 0.55:0.45 and 0.725:0.275.

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 · C6. 0.1 M Bicine pH 9.0, 20% PEG 6000 D1. 0.1 M Citric Acid pH 4.0, 30% PEG 6000 D2. 0.1 M Citric Acid pH 5.0, 30% PEG 6000 D3. 0.1 M MES pH 6.0, 30% PEG 6000 D4. 0.1 M HEPES pH 7.0, 30% PEG 6000 D5. 0.1 M Tris pH 8.0, 30% PEG 6000 D6. 0.1 M Bicine pH 9.0, 30% PEG 6000. Author: Sam Last modified by: Sam

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